Manure sampling and nutrient analysis

Manure is a valuable source of nutrients for crops. Testing manure for nutrient content helps meet crop nutrient needs efficiently. This leads to increased profit and decreased risk of pollution. Nutrient estimation tables give a general idea of nutrient content, but they tend to differ from actual values due to factors like storage type and animal diet. Therefore, we don’t recommend you rely on those tables. The most accurate way to manage manure for nutrients is to analyze for nutrient content.

Manure uniformity

Nutrient content in manure varies from one area to another. Solids tend to settle to the bottom of liquid storage systems. Solid storage systems vary based on bedding content and time of stacking. It is important to make the manure as uniform as possible so that the applied rate is accurate.

Use a pit agitator to mix liquid manure to make it more uniform. The solid portion of the manure will begin to settle to the bottom right after agitation. Solid manure is more difficult to make uniform. When piling the manure, alternate between areas with large amounts of bedding and areas of small amounts of bedding.

How to sample manure for nutrient analysis

Manure sampling timing can change the accuracy of a manure test. We recommend taking the sample at manure application. The main drawback of this method is that you cannot use the test results to adjust application rates for the current year. However, the results will help with future fertilizer rate calculations. Keeping detailed records of manure test results will allow for accurate rates in the following years.

Sampling in storage and before manure application allows time to receive results and adjust rates in the current season. However, nutrients are lost with further storage and handling, so it may not give an accurate picture of the nutrients applied. This is particularly true for farms with large amounts of livestock and manure since collecting a representative sample of the manure may not be easy to do.

Manure should be tested each year for the first three years of operation; then every three or four years. Also test whenever management practices change that could alter nutrient content, like the storage system or feed. The Minnesota Pollution Control Agency (MPCA) requires farms with over 100 animal units to test manure at least once every four years. Visit the MPCA website for more information.

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Sampling liquid or slurry manure during spreading

Sampling liquid or slurry manure when it is applied is probably the safest and most accurate sampling method:

  1. Collect many samples from the spreader or during pit pumping and combine them in a clean plastic bucket.
  2. Stir the manure ensuring that any solids are suspended.
  3. Subsample from this mixture quickly before solids settle out.
  4. Place subsample in a well-labeled, plastic, wide-mouth container with a screw-top lid. Leave some air space near the top of the container. Do not use glass containers as they can break in response to gas expansion.
  5. If the sample must be mailed to the testing laboratory, freeze the sample and place it in a sealed plastic bag.

During sampling, wear gloves and appropriate personal protective equipment. Send all manure samples to a testing laboratory as soon as possible after sampling to minimize nutrient losses. Visit the Minnesota Department of Agriculture website for a list of certified manure testing laboratories.

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Sampling liquid or slurry from a deep pit

Liquid manure may also be sampled from deep pits prior to land application, though safety precautions should be taken to avoid harmful gases.

  1. Build a manure collector, which consists of a PVC pipe cut to a length that would reach the bottom of the pit. Attach a rubber ball to a wire and string the wire through the pipe, so that you can pull it shut when you are ready to collect your sample.
  2. Lower the PVC pipe into the pit and when it hits the bottom, pull the wire to shut the pipe with the rubber ball. Pull the pipe from the pit and empty the sample into a clean, 5-gallon bucket.
  3. Collect several samples this way and try to sample from several pit access ports, if possible.
  4. Stir the manure in the bucket, ensuring that any solids are suspended.
  5. Subsample from this mixture quickly before solids settle out.
  6. Place the subsample in a well-labeled, plastic, wide-mouth container with a screw-top lid. Leave some air space near the top of the container. Do not use containers, as they can break in response to gas expansion.
  7. If the sample must be mailed to the testing laboratory, freeze the sample and place in a sealed plastic bag.

During sampling, wear gloves and appropriate personal protective equipment. Send all manure samples to a testing laboratory as soon as possible after sampling to minimize nutrient losses. Visit the Minnesota Department of Agriculture website for a list of certified manure testing laboratories.

Watch the video for more tips

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Sampling solid manure

Solid manure varies in nutrient content more than liquid manure across storage. Therefore, the key to accuracy is sampling at many sites.

  1. Collect multiple samples from various places in the manure pile and place them in a clean plastic bucket.
    1. If collecting during application, sample from each load to represent the beginning and end of application.
    2. If collecting from storage, avoid sampling from the top or edges of the pile where a crust has formed.

    During sampling, wear gloves and appropriate personal protective equipment. Send all manure samples to a testing laboratory as soon as possible after sampling to minimize nutrient losses. Visit the Minnesota Department of Agriculture website for a list of certified manure testing laboratories.

    Watch the video for more tips

    Although it's geared toward small livestock farms, the principles apply to all sizes of farms.

    Understanding a manure analysis output

    Choosing which manure tests to do depends on individual needs and concerns. At the very least, measure total nitrogen (N), total phosphorus (P), total potassium (K), and moisture content. We also highly recommend having your manure tested for ammonium nitrogen (NH4-N) content. Please note that none of the nutrients in manure are 100% available the first year. To calculate the amount that is plant available, see Manure Characteristics.